LC-D100藍寶石光電化學反應釜

       北京(jing)世(shi)紀森朗(lang)公司LightChem系(xi)列光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)藍寶石(shi)反應(ying)(ying)(ying)釜(fu)，也(ye)稱(cheng)光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)聯(lian)合(he)(he)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)高(gao)壓(ya)反應(ying)(ying)(ying)釜(fu)，是(shi)在高(gao)壓(ya)光(guang)(guang)(guang)(guang)(guang)(guang)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)反應(ying)(ying)(ying)釜(fu)與高(gao)壓(ya)電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)反應(ying)(ying)(ying)釜(fu)基(ji)礎上(shang)開發出來的(de)。是(shi)結合(he)(he)高(gao)壓(ya)光(guang)(guang)(guang)(guang)(guang)(guang)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)反應(ying)(ying)(ying)釜(fu)及(ji)高(gao)壓(ya)電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)反應(ying)(ying)(ying)釜(fu)特(te)點，實現高(gao)溫高(gao)壓(ya)情況下光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)聯(lian)合(he)(he)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)反應(ying)(ying)(ying)。光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)反應(ying)(ying)(ying)釜(fu)，就是(shi)用(yong)光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)協(xie)同作用(yong)提高(gao)光(guang)(guang)(guang)(guang)(guang)(guang)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)材料(liao)的(de)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)活(huo)(huo)性，光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)測試(shi)(shi)本質為一(yi)(yi)(yi)種光(guang)(guang)(guang)(guang)(guang)(guang)輔(fu)助下的(de)電(dian)(dian)(dian)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)測試(shi)(shi)，電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)中的(de)基(ji)本原理和方法在PEC中大部(bu)分適用(yong)。光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)測試(shi)(shi)系(xi)統一(yi)(yi)(yi)般分為光(guang)(guang)(guang)(guang)(guang)(guang)源、反應(ying)(ying)(ying)系(xi)統（三電(dian)(dian)(dian)極+反應(ying)(ying)(ying)器）、測試(shi)(shi)系(xi)統（電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)工作站+色譜(pu)）三個部(bu)分。將催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)固定(ding)在導電(dian)(dian)(dian)基(ji)體上(shang)，同時外(wai)加偏(pian)壓(ya)抑制(zhi)光(guang)(guang)(guang)(guang)(guang)(guang)生(sheng)(sheng)電(dian)(dian)(dian)子和空(kong)穴(xue)的(de)復合(he)(he)，從而發展出一(yi)(yi)(yi)種新型的(de)技術(shu)(shu)—電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)輔(fu)助光(guang)(guang)(guang)(guang)(guang)(guang)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)技術(shu)(shu)，即光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)技術(shu)(shu)。這是(shi)一(yi)(yi)(yi)種有效(xiao)促進(jin)光(guang)(guang)(guang)(guang)(guang)(guang)生(sheng)(sheng)電(dian)(dian)(dian)子和空(kong)穴(xue)分離，并利用(yong)光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)協(xie)同作用(yong)增(zeng)強光(guang)(guang)(guang)(guang)(guang)(guang)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)氧化(hua)(hua)(hua)(hua)(hua)技術(shu)(shu)，以光(guang)(guang)(guang)(guang)(guang)(guang)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)作為光(guang)(guang)(guang)(guang)(guang)(guang)陽(yang)極，對其施加一(yi)(yi)(yi)定(ding)的(de)偏(pian)壓(ya)，光(guang)(guang)(guang)(guang)(guang)(guang)生(sheng)(sheng)電(dian)(dian)(dian)子就會遷移至外(wai)電(dian)(dian)(dian)路，從而抑制(zhi)光(guang)(guang)(guang)(guang)(guang)(guang)生(sheng)(sheng)電(dian)(dian)(dian)子和空(kong)穴(xue)的(de)復合(he)(he)，空(kong)穴(xue)在催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)表面積累，并進(jin)一(yi)(yi)(yi)步提高(gao)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)劑(ji)的(de)活(huo)(huo)性。光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)還(huan)原CO2，半導體在光(guang)(guang)(guang)(guang)(guang)(guang)照作用(yong)下，利用(yong)陰(yin)極材料(liao)在電(dian)(dian)(dian)化(hua)(hua)(hua)(hua)(hua)學(xue)(xue)作用(yong)下都能產(chan)生(sheng)(sheng)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)活(huo)(huo)性的(de)特(te)性，達到(dao)光(guang)(guang)(guang)(guang)(guang)(guang)電(dian)(dian)(dian)結合(he)(he)催(cui)(cui)(cui)(cui)化(hua)(hua)(hua)(hua)(hua)還(huan)原CO2的(de)目的(de)。

LC-D100藍寶石電(dian)化(hua)學高壓反應釜技(ji)術參數：

 LightChem系列光電化學藍寶石(shi)反(fan)應釜， 視窗(chuang)材質采用(yong)藍寶石(shi)玻璃，可視直徑(jing)40MM。電化學電極(ji)標配三電極(ji)體(ti)系：工作電極(ji)，參比電極(ji)，輔助電極(ji)。溫度250度。壓力(li)10Mpa、20Mpa、30Mpa可選。世紀(ji)森(sen)朗MRSC-LC反(fan)應釜控制系統V1.06，可以實(shi)現對反(fan)應釜的加熱(re)、冷卻、攪拌、程(cheng)序(xu)編(bian)程(cheng)、數(shu)據采集等諸多控制功能。  

1、 MRSC-LC-D反應釜控制系(xi)統V1.06控溫(wen)檢測：

液晶顯示(shi)屏三色LCD智能控(kong)制儀，同(tong)時檢(jian)測釜內溫度(du)(du)和釜壁溫度(du)(du)。并(bing)進行連(lian)鎖控(kong)制，任何一路超過(guo)設(she)定(ding)值均不會加(jia)熱(re)，并(bing)且可以自(zi)行設(she)定(ding)加(jia)熱(re)速率。這樣有效防止了溫度(du)(du)過(guo)沖(chong)，非(fei)常(chang)適(shi)合反應(ying)溫度(du)(du)低于150度(du)(du)的實驗(yan)和需要(yao)限制一些超過(guo)臨界溫度(du)(du)值會產(chan)生爆炸或分解的反應(ying)物質。

2、高(gao)溫磁子(zi)強力攪(jiao)拌，可配置槳式機械攪(jiao)拌方式：

光電(dian)聯(lian)合催化反應釜采用稀土(tu)材(cai)料強力磁鐵，攪拌(ban)力矩大大提(ti)升。直流無刷電(dian)機(ji)使攪拌(ban)壽命理(li)論上可(ke)以達到10年(nian)以上而不(bu)需更換磨損部(bu)件。轉速可(ke)以由0-1500轉/分自由設定(ding)，且不(bu)失轉。

3、聲光雙重報警(jing)系(xi)統：

溫度或壓力報(bao)(bao)警(jing)(jing)后(hou)(hou)均(jun)會(hui)觸發報(bao)(bao)警(jing)(jing)，報(bao)(bao)警(jing)(jing)后(hou)(hou)相關報(bao)(bao)警(jing)(jing)點顯示為(wei)紅(hong)色并(bing)(bing)且閃(shan)爍。控制(zhi)器內(nei)置交流(liu)接觸器，控制(zhi)加熱(re)電(dian)源開關。報(bao)(bao)警(jing)(jing)同時加熱(re)自(zi)動停(ting)止。連鎖控制(zhi)后(hou)(hou)，此報(bao)(bao)警(jing)(jing)需人為(wei)檢查后(hou)(hou)找到故(gu)障原因后(hou)(hou)方(fang)可手動恢復(fu)。（也(ye)可設(she)定為(wei)自(zi)動恢復(fu)加熱(re)）并(bing)(bing)可選配可燃氣體報(bao)(bao)警(jing)(jing)系統(tong)。

4、模(mo)塊化加熱(re)設計：

光(guang)電聯(lian)合(he)催化反(fan)應(ying)釜不同(tong)的容積(ji)的反(fan)應(ying)釜可以共用(yong)控制底(di)盤，相同(tong)外徑的釜體可以共用(yong)加(jia)熱器(qi)。從而大大節省了經費。并且加(jia)熱器(qi)外殼設有專(zhuan)用(yong)防燙護罩(zhao)，防止客戶燙傷(shang)。

5、靈活的選配及定(ding)制：世(shi)紀森朗擁(yong)有著(zhu)十多(duo)年微(wei)型高壓反應釜(fu)加(jia)工技(ji)術(shu)經驗(yan)和反應設(she)備(bei)核心技(ji)術(shu)，可(ke)為(wei)用戶定(ding)制加(jia)工適(shi)應不(bu)同實驗(yan)體系的反應設(she)備(bei)，并保證其安(an)全、穩定(ding)、操作簡便：

     a、氣(qi)體(ti)報警(jing)系統：配備氣(qi)體(ti)報警(jing)系統后，可燃氣(qi)體(ti)報警(jing)后會聯動(dong)反應(ying)釜控制器報警(jing)，并且加(jia)熱自(zi)動(dong)停止(zhi)。

     b、壓力顯(xian)(xian)示（控(kong)制）模塊(kuai)：壓力顯(xian)(xian)示模塊(kuai)包(bao)含壓力傳感(gan)器、連接電纜、智能顯(xian)(xian)示控(kong)制器。壓力控(kong)制模塊(kuai)額(e)外添加氣(qi)動背壓閥及電子(zi)壓力控(kong)制器。壓力范圍視反應(ying)釜耐(nai)壓配置(zhi)。

     c 、冷卻(que)模塊(kuai)：可以選配氣動冷卻(que)模塊(kuai)快速冷卻(que)釜壁溫度。包含電(dian)纜、電(dian)磁閥、及管線。

     d、選配數據(ju)通(tong)訊電纜及數據(ju)采集(ji)軟件。可以實現對(dui)光電聯(lian)合催化磁(ci)力反(fan)(fan)應(ying)釜反(fan)(fan)應(ying)溫度、釜壁(bi)溫度和壓力的采集(ji)。

  e、相關數據可(ke)以動態回(hui)放(fang)，可(ke)以同時(shi)記錄所有數據，并(bing)可(ke)以為(wei)反應釜配套系統(tong)添(tian)加額(e)外的保溫伴(ban)熱(re)模(mo)塊或(huo)壓力(li)顯示模(mo)塊。數據可(ke)以轉換(huan)為(wei)excel表格，方便(bian)客戶進行二次圖表處理。

鑄就(jiu)實驗室(shi)反應(ying)(ying)釜(fu)主流影響力，助力中國科研(yan)事業發(fa)展。世紀(ji)森朗擁有著(zhu)十多年(nian)微型(xing)高(gao)壓(ya)反應(ying)(ying)釜(fu)加(jia)工技術(shu)經驗和(he)反應(ying)(ying)設備(bei)核心技術(shu)，可(ke)為用(yong)戶定制加(jia)工適應(ying)(ying)不同實驗體系的反應(ying)(ying)設備(bei)，并保(bao)證其安全、穩定、操作簡便(bian)。