視窗聚合(he)反(fan)應(ying)釜技術(shu)參數:
1、密封性要好,無(wu)泄漏、安(an)全,并在材料(liao)(liao)處理的實驗過程中(zhong),材料(liao)(liao)受熱均勻;
2、其(qi)次要求(qiu)(qiu)控制系統準確有(you)效(xiao)(xiao),安全可靠,實(shi)用的數據采集都要求(qiu)(qiu)及時,方便,有(you)效(xiao)(xiao);
3、夾套型釜(fu)體帶(dai)有(you)(you)雙面長(chang)(chang)條視(shi)窗,視(shi)窗尺寸:長(chang)(chang)度(du)(du)不(bu)(bu)小于(yu)(yu)89mm,寬度(du)(du)不(bu)(bu)小于(yu)(yu)16mm;釜(fu)體容(rong)積:不(bu)(bu)小于(yu)(yu)1000mL;為能夠使物料(liao)反應(ying)混合均勻,釜(fu)內溫(wen)度(du)(du)梯度(du)(du)小,長(chang)(chang)徑比大于(yu)(yu)1.3;帶(dai)有(you)(you)底部無死角卸料(liao)閥,直徑為3/8英寸,不(bu)(bu)銹鋼材質;
4、溫度:不小(xiao)于(yu)200℃,壓力:不小(xiao)于(yu)120 bar;
5、加工工藝及(ji)材(cai)質(zhi)(zhi)(zhi):反(fan)應(ying)(ying)(ying)釜(fu)(fu)體、釜(fu)(fu)頭(tou)、內部構件(jian)等應(ying)(ying)(ying)采(cai)用(yong)相(xiang)同(tong)材(cai)質(zhi)(zhi)(zhi),避免因材(cai)質(zhi)(zhi)(zhi)不同(tong)而(er)發生(sheng)的(de)電化學反(fan)應(ying)(ying)(ying),選擇(ze)不銹鋼材(cai)質(zhi)(zhi)(zhi);為(wei)避免焊接腐蝕、保證受壓均(jun)勻(yun),釜(fu)(fu)體、釜(fu)(fu)頭(tou)應(ying)(ying)(ying)采(cai)用(yong)整體棒材(cai)切(qie)割工藝,保證釜(fu)(fu)頭(tou)、釜(fu)(fu)體無任何焊接點;驅(qu)動方(fang)(fang)式(shi):為(wei)了(le)能使物料攪拌(ban)均(jun)勻(yun),應(ying)(ying)(ying)采(cai)用(yong)帶有(you)攪拌(ban)桿及(ji)攪拌(ban)槳式(shi)的(de)機(ji)(ji)械攪拌(ban)形(xing)式(shi),且(qie)需要(yao)配有(you)冷(leng)卻水夾套,為(wei)防(fang)止泄露(lu)應(ying)(ying)(ying)采(cai)用(yong)磁力密(mi)(mi)封(feng)。根據物料性(xing)質(zhi)(zhi)(zhi)以(yi)及(ji)滿足以(yi)后(hou)拓展性(xing)的(de)需要(yao),驅(qu)動電機(ji)(ji)功率應(ying)(ying)(ying)不小于0.5馬(ma)力,扭矩不小于58英寸-磅。為(wei)滿足試驗需求(qiu),轉速為(wei)0-700轉/分鐘,且(qie)能夠進行無級調(diao)速。密(mi)(mi)封(feng)方(fang)(fang)式(shi):為(wei)保證反(fan)應(ying)(ying)(ying)釜(fu)(fu)使用(yong)安全,不能用(yong)法蘭式(shi)密(mi)(mi)封(feng)方(fang)(fang)式(shi),建議采(cai)用(yong)墊片式(shi)密(mi)(mi)封(feng)墊片,快開式(shi)抱環(huan)密(mi)(mi)封(feng)結構,并且(qie)抱環(huan)的(de)材(cai)質(zhi)(zhi)(zhi)應(ying)(ying)(ying)選擇(ze)耐(nai)高溫、高強度的(de)金屬材(cai)質(zhi)(zhi)(zhi);
釜頭設計要求:應(ying)(ying)帶有(you)(you)能(neng)(neng)夠(gou)(gou)便(bian)(bian)于(yu)直(zhi)接觀(guan)察(cha)的(de)(de)(de)機(ji)(ji)械式指針壓(ya)力表,為(wei)(wei)(wei)方便(bian)(bian)觀(guan)察(cha)及(ji)對比(bi),表盤刻度(du)至(zhi)少有(you)(you)2種不同(tong)單(dan)位,其(qi)中一種單(dan)位應(ying)(ying)為(wei)(wei)(wei)psi;應(ying)(ying)帶有(you)(you)直(zhi)接單(dan)獨(du)安(an)(an)裝在釜頭(tou)上的(de)(de)(de)安(an)(an)全防(fang)腐防(fang)爆(bao)(bao)膜,且隨機(ji)(ji)文件(jian)(jian)中應(ying)(ying)有(you)(you)安(an)(an)全防(fang)爆(bao)(bao)膜有(you)(you)關的(de)(de)(de)計算公(gong)式等(deng)證明材(cai)(cai)料,為(wei)(wei)(wei)避免因受腐蝕而(er)影響耐壓(ya),防(fang)爆(bao)(bao)膜應(ying)(ying)選(xuan)用防(fang)腐合金材(cai)(cai)質防(fang)爆(bao)(bao)膜;應(ying)(ying)帶有(you)(you)能(neng)(neng)夠(gou)(gou)實(shi)時(shi)(shi)測量釜內(nei)溫(wen)度(du)的(de)(de)(de)熱(re)電偶,用于(yu)反應(ying)(ying)溫(wen)度(du)的(de)(de)(de)測定;應(ying)(ying)具備(bei)實(shi)驗過程(cheng)中進(jin)氣、取(qu)氣、取(qu)液功(gong)能(neng)(neng)及(ji)相(xiang)配(pei)套的(de)(de)(de)閥門;應(ying)(ying)具備(bei)實(shi)驗過程(cheng)中或結束后對反應(ying)(ying)釜內(nei)壓(ya)力的(de)(de)(de)降低或排空相(xiang)應(ying)(ying)的(de)(de)(de)閥門;增加1個開口,配(pei)有(you)(you)閥門,備(bei)用于(yu)進(jin)氣;控(kong)制系統:應(ying)(ying)選(xuan)用先進(jin)的(de)(de)(de)控(kong)制器(qi),應(ying)(ying)不低于(yu)以下(xia)功(gong)能(neng)(neng):能(neng)(neng)夠(gou)(gou)實(shi)時(shi)(shi)顯(xian)(xian)示(shi)(shi)釜內(nei)溫(wen)度(du),可進(jin)行數(shu)(shu)據采(cai)集,溫(wen)度(du)顯(xian)(xian)示(shi)(shi)精度(du)為(wei)(wei)(wei)0.1°C; 能(neng)(neng)夠(gou)(gou)實(shi)時(shi)(shi)顯(xian)(xian)示(shi)(shi)釜內(nei)壓(ya)力,并(bing)帶有(you)(you)超壓(ya)保護功(gong)能(neng)(neng),一旦超過預先設定的(de)(de)(de)安(an)(an)全壓(ya)力,會(hui)有(you)(you)光報警提醒,并(bing)切斷電源,且可實(shi)現數(shu)(shu)據采(cai)集;能(neng)(neng)夠(gou)(gou)實(shi)時(shi)(shi)顯(xian)(xian)示(shi)(shi)轉速,并(bing)能(neng)(neng)夠(gou)(gou)在控(kong)制器(qi)及(ji)PC機(ji)(ji)上實(shi)時(shi)(shi)控(kong)制和數(shu)(shu)據采(cai)集;控(kong)制器(qi)應(ying)(ying)能(neng)(neng)夠(gou)(gou)與PC機(ji)(ji)連接,能(neng)(neng)夠(gou)(gou)實(shi)時(shi)(shi)的(de)(de)(de)控(kong)制溫(wen)度(du)、轉速,并(bing)能(neng)(neng)夠(gou)(gou)實(shi)時(shi)(shi)收集及(ji)儲存溫(wen)度(du)、轉速、壓(ya)力等(deng)數(shu)(shu)據;其(qi)他配(pei)套組件(jian)(jian):易(yi)損備(bei)件(jian)(jian)一套。